ZrO2陶瓷生坯表面微织构制备工艺的研究
2018-02-02
作者:刘亚运1,刘莉莉2,邓建新1,王伟1,葛栋良1,张贵梁1 单位:1山东大学;2河南科技学院
摘要:通过冷等静压技术制备ZrO2陶瓷生坯,并利用脉冲激光在陶瓷生坯表面制备微织构沟槽。探究激光参数对表面微织构质量的影响,并研究烧蚀区域的热影响区和激光烧蚀表面的微观形态变化。实验结果表明:通过激光加工可以在ZrO2陶瓷生坯表面加工出深度30-50μm、宽度15-50μm质量较好的微织构沟槽;激光参数对表面加工质量有较大的影响,激光频率低于40Hz、功率低于6W和扫描速度高于200mm/s能够获得较好的表面质量;当激光频率高于60Hz、功率高于10W和扫描速度低于150mm/s时,在激光烧蚀表面容易形成烧蚀层,分析得知烧蚀层是由于在激光高温照射下ZrO2颗粒的熔化和再凝固形成的。
关键词:陶瓷生坯;激光加工;表面质量;烧蚀微观形貌
中图分类号:TG174.4;TH161文献标志码:A
Fabrication of MicroScale Textured Grooves on Green ZrO2
Ceramics by Pulsed Laser Ablation
Liu Yayun,Liu Lili,Deng Jianxin,Wang Wei,Ge Dongliang,Zhang Guiliang
Abstract:The green ZrO2 ceramics are fabricated by cold isostatic pressing.Pulsed laser ablation is performed to fabricate microscale textured grooves on the surface of green ZrO2 ceramics. The influence of laser parameters on surface quality is studied. The heataffected zone around the machined grooves and micro morphology of laserirradiated surface are investigated. The results show that microscale textured grooves with a width of 3050μm and a depth of 1550μm on the green ZrO2 ceramic surfaces are successfully fabricated by pulsed laser ablation. The laser parameters has a profound influence on the surface quality of microscale textured grooves.Better surface quality could be obtained with frequency below 40 Hz,power below 6 W,and scanning velocity above 200 mm/s. A sintering layer is found on the laserirradiated surfaces when frequency is above 60 Hz,power is above 10 W,and scanning velocity is below 150 mm/s. Analysis of this sintering layer revealed clear melting and resolidification of ZrO2 particles.
Keywords:green ceramics;laser machining;surface quality;micromorphology of laser ablation